Analytic chemistry II with lab

A.Y. 2019/2020
Lesson for
12
Max ECTS
136
Overall hours
SSD
CHIM/01
Language
Italian
Learning objectives
Instrumentations and fundamentals of main analytical and separation techniques. Qualitative and quantitative problem solving.
At the end of the course the student will be able to solve qualitative and quantitative analytical problems with the most suitable technique. He will develop the expertise to characterize simple organic structure from the corresponding IR, NMR and MS spectra.

Course structure and Syllabus

Active edition
Yes
Responsible
Modulo: Chimica Analitica II
CHIM/01 - ANALYTICAL CHEMISTRY - University credits: 6
Lessons: 48 hours
Professor: Prati Laura
Modulo: Laboratorio di Chimica Analitica II
CHIM/01 - ANALYTICAL CHEMISTRY - University credits: 6
Practicals: 48 hours
Laboratories: 32 hours
Lessons: 8 hours
Shifts:
Corso A
Professor: Guglielmi Vittoria
Corso B
Professor: Guglielmi Vittoria
Modulo: Laboratorio di Chimica Analitica II
Syllabus
Qualitative and quantitative experiences on the main spectroscopic (AAS, AES, UV-Vis, IR, fluorescence) and chromatographic (GC, HPLC) techniques presented during the lectures.
Modulo: Chimica Analitica II
Syllabus
Course content
Principles of spectrophotometric and photoelectronic methods. Atomic adsorption and emission. Molecular spectroscopy: UV-vis, IR and Raman, fluorescence and phosphorescence.
Mass spectrometry.
Nuclear Magnetic Resonance: monodimensional 1H- and 13C-NMR techniques. Spectrum parameter analyses: chemical shift and coupling constant. Overhauser effect.
Principles and methods of chromatographic techniques (GC and HPLC).
Set-up of qualitative and quantitative analyses.
Exercises on structure disclosing based on NMR, IR, UV and MS spectra. Practices of theoretical concepts. Numerical exercises on quantitative analyses involving spectroscopic and chromatographic techniques.

Suggested prerequisites
Positive assessment of analytical chemistry I

Reference material
- Holler, Skoog, Crouch "Chimica Analitica Strumentale" EdiSES, VCH;
- R.M. Silverstein, F.X. Webster, Identificazione spettroscopica di composti organici, Ed. CEA,
- lecture notes.

Assessment method [required] (use at least 2 lines):
The exam will be constitute by:
- Written test of 5 questions/exercises based on exercises and laboratory experiments
- Written test divided into two parts:
o 6 questions of short solution which, only if correctly solved, allow to pass to the second part
o 5 questions on theory and spectra interpretation
The two tests will be held in different day but they will be assessed with a single mark.

Language of instruction
Italian

Attendance Policy
Strongly suggested, compulsory frequency at the laboratory

Mode of teaching
Traditional

Website
ARIEL
Lesson period
First semester
Assessment methods
Esame
Assessment result
voto verbalizzato in trentesimi