Analytic chemistry II with lab

A.Y. 2020/2021
12
Max ECTS
136
Overall hours
SSD
CHIM/01
Language
Italian
Learning objectives
Instrumentations and fundamentals of main analytical and separation techniques. Qualitative and quantitative problem solving.
Expected learning outcomes
At the end of the course the student will be able to solve qualitative and quantitative analytical problems with the most suitable technique. He will develop the expertise to characterize simple organic structure from the corresponding IR, NMR and MS spectra.
Course syllabus and organization

Single session

Responsible
Lesson period
First semester
Lectures and exercises will be held on the Zoom platform, will be in synchronous mode based on the timetable and can also be followed asynchronously because they are recorded and left available to students.
Prerequisites for admission
Fundamentals of General Chemistry and Organic Chemistry I
Assessment methods and Criteria
-The exam will be constitute by:
- Written test of 5 questions/exercises based on exercises and laboratory experiments
- Written test divided into two parts:
o 6 questions of short solution which, only if correctly solved, allow to pass to the second part
o 5 questions on theory and spectra interpretation
The two tests will be held in different day but they will be assessed with a single mark.
Modulo: Laboratorio di Chimica Analitica II
Course syllabus
Qualitative and quantitative experiences on the main spectroscopic (AAS, AES, UV-Vis, IR, fluorescence) and chromatographic (GC, HPLC) techniques presented during the lectures.
Nuclear Magnetic Resonance: monodimensional 1H- and 13C-NMR techniques. Spectrum parameter analyses: chemical shift and coupling constant. Overhauser effect.
Teaching methods
Practice exercises in classroom and laboratory
Teaching Resources
Holler, Skoog, Crouch "Chimica Analitica Strumentale" EdiSES, VCH;
A.Randazzo "Guida pratica all'interpretazione di spettri NMR" Loghia Ed
Lecture notes
Modulo: Chimica Analitica II
Course syllabus
Principles of spectrophotometric and photoelectronic methods. Atomic adsorption and emission. Molecular spectroscopy: UV-vis, IR and Raman, fluorescence and phosphorescence.
Mass spectrometry.
Principles and methods of chromatographic techniques (GC and HPLC).
Set-up of qualitative and quantitative analyses.
Exercises on structure disclosing based on IR, UV and MS spectra. Practices of theoretical concepts. Numerical exercises on quantitative analyses involving spectroscopic and chromatographic techniques.
Teaching methods
Lessons and interactive discussion
Teaching Resources
- Holler, Skoog, Crouch "Chimica Analitica Strumentale" EdiSES, VCH;
- R.M. Silverstein, F.X. Webster, Identificazione spettroscopica di composti organici, Ed. CEA,
- lecture notes.
Modulo: Chimica Analitica II
CHIM/01 - ANALYTICAL CHEMISTRY - University credits: 6
Lessons: 48 hours
Professor: Prati Laura
Modulo: Laboratorio di Chimica Analitica II
CHIM/01 - ANALYTICAL CHEMISTRY - University credits: 6
Practicals: 48 hours
Laboratories: 32 hours
Lessons: 8 hours
Shifts:
Corso A
Professor: Guglielmi Vittoria
Corso B
Professor: Guglielmi Vittoria
Professor(s)
Reception:
By appointment
Department of Chemistry, via Golgi 19 - Milano